毕业设计（论文）题目：金属氧化物掺杂C3N4/TiO2光储阴极的抗腐蚀性能研究

一、毕业设计（论文）内容及要求（包括原始数据、技术要求、达到的指标和应做的实验等）

(1)查找相关资料，调研涂层的制备方法及性能原理测试等相关知识。

(2)准备涂层制备及测试所需的的实验药品设备，搭置自制实验装置，制备涂层并测试涂层防腐蚀性能。

(3)获得论文所需要的抗蚀性数据如电化学测试分析图谱及相关的结构物相分析图。

(4)根据相关的实验数据对金属氧化物掺杂的C3N4/TiO2涂层进行结构分析与耐蚀性评估。

(5)撰写毕业设计论文。

二、完成后应交的作业（包括各种说明书、图纸等）

1.毕业设计论文一份（不少于1.5万字）；

2.外文译文一篇（不少于5000英文单词）；

三、完成日期及进度起止时间：第一周~第十五周（2017.2.20～6.2）

1.文献检索与阅读2周：（第一周～第二周）（2.20～3.3）

2.设计与实验10周：（第三周～第十二周）（3.6~5.12）

3.撰写论文及评阅2周：（第十三周～第十四周）（5.15~5.26）

4.答辩1周：（第十五周）（5.29~6.2）主要参考资料（包括书刊名称、出版年月等）：

[1] Guo Y.X., He J.P. *, Wu S.C., Wang T., Li G.X., Hu Y.Y., Xue

H.R ., Sun X., Tang J.，Liu M.Z. ;Effects of platinum on photo-assisted electrocatalytic activity of fringe-shaped highly ordered mesoporous Titanium dioxide film, J.Power Sources, 2012,208:58-66.

[2] Liu J., Liu N.Y.,Li H.,Wang L.P..,Wu X.Q.,Lifshitz Y., Kang Z.H.,A critical study of the generality of the two step two electron pathway for water splitting by application of a C3N4/MnO2 photocatalyst,Nanoscale, 2016, 8:11956–11961.

[3] Xu Jie, Shang J.K., Jiang Q,WangY,Li,Y.X.,Facile alkali-assisted synthesis of g-C3N4 materials and their high-performance catalytic application in solvent-free cycloaddition of CO2 to epoxides, RSC Adv., 2016, 6:55382–55392.

[4] Shiraishi Y.,Kanazawa S.,Sugano Y.,Tsukamoto D.,HSakamoto I.,Ichikawa S. ,Hirai T.,David M.T., Highly Selective Production of Hydrogen Peroxide on Graphitic Carbon Nitride (g C3N4) PhotocatalystActivated by Visible Light ,ACS Catal. 2014, 4:774 780.

[5] Bu Y.,Chen Z.Y.,Yu J.Q.,Li W.B.,A novel application of g-C3N4 thin film in photoelectrochemical anticorrosion, Electrochimica Acta, 2013,88:294300.

[6] Wang J.,Zhang W.D., Modification of TiO2 nanorod arrays by graphite-like C3N4 with high visible light photoelectrochemical activity, Electrochimica Acta, 2012,71:1016.

[7] Chang F.,Zhang J.,Xie Y.C.,Chen J.,Li C.L.,Wang J.,Luo J.R.,DengB.Q. ,Hu X.F.,Fabrication, characterization, and photocatalytic performance of exfoliated g-C3N4TiO2 hybrids Applied Surface Science 2014,311:574581.

[8] Wang J.X.,Huang J.,Xie H.L.,Qu A.,Synthesis of g-C3N4/TiO2 with enhanced.photocatalytic activity for H2 evolution by a simple method, International journal of hydrogen energy, 2014,39:6354-6363.

[9] He F.,Chen G.,Yu Y.G.,Hao S.,Zhou Y.S.,Zheng Y.,Facile Approach to Synthesize g PAN/g C3N4 Composites withEnhanced Photocatalytic H2 Evolution Activity,Applied Materials & Interfaces, 2014,6:7171 7179.